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Methyl 4-(butyrylamino)-3-methyl-5-nitrobenzoate
- Name Methyl 4-(butyrylamino)-3-methyl-5-nitrobenzoate
- CAS 152628-01-8
- Purity 99%
Product Details
Factory Sells Best Quality Methyl 4-(butyrylamino)-3-methyl-5-nitrobenzoate 152628-01-8 with steady supply
- Molecular Formula: C13H16N2O5
- Molecular Weight: 280.28
- Appearance/Colour: An off-white to Cream-colored powder
- Vapor Pressure: 0mmHg at 25°C
- Refractive Index: 1.572
- Boiling Point: 468.052 °C at 760 mmHg
- PKA: 13.27±0.70(Predicted)
- Flash Point: 236.87 °C
- PSA： 101.22000
- Density: 1.265 g/cm3
- LogP: 3.02460
Methyl 4-(butyrylamino)-3-methyl-5-nitrobenzoate(Cas 152628-01-8) Usage
InChI:InChI=1/C13H16N2O5/c1-4-5-11(16)14-12-8(2)6-9(13(17)20-3)7-10(12)15(18)19/h6-7H,4-5H2,1-3H3,(H,14,16)
152628-01-8 Relevant articles
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152628-01-8 Process route
-
-
301533-59-5
methyl 4-(n-butyrylamino)-3-methylbenzoate
-
-
4-butyrylamino-3-methyl-2-nitrobenzoic acid methyl ester
-
-
4-butyrylamino-3-methyl-6-nitrobenzoic acid methyl ester
-
-
152628-01-8
4-butyrylamino-3-methyl-5-nitro-benzoic acid methyl ester
| Conditions | Yield |
|---|---|
|
methyl 4-(n-butyrylamino)-3-methylbenzoate;
With
sulfuric acid;
at 20 ℃;
With
sulfuric acid; nitric acid;
at -10 - 0 ℃;
for 2h;
|
89%
|
|
With
sulfuric acid; nitric acid;
In
water;
at -10 - 10 ℃;
for 2.75 - 3.25h;
|
88%
|
-
-
18595-14-7
methyl 4-amino-3-methylbenzoate
-
-
152628-01-8
4-butyrylamino-3-methyl-5-nitro-benzoic acid methyl ester
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: 79.6 percent / triethylamine / CH2
Cl2
/ 1 h / 20 °C
2: 75.6 percent / nitric acid / 1.5 h / -20 - -15 °C
With
nitric acid; triethylamine;
In
dichloromethane;
|
|
|
Multi-step reaction
with
2
steps
1: chlorobenzene / 100 °C
2: fuming HNO3
, 60percent H2
SO4
/ 0 °C
With
sulfuric acid; nitric acid;
In
chlorobenzene;
|
|
|
Multi-step reaction
with
2
steps
1: triethylamine / dichloromethane / 0 °C
2: sulfuric acid; nitric acid
With
sulfuric acid; nitric acid; triethylamine;
In
dichloromethane;
|
|
|
Multi-step reaction
with
2
steps
1: triethylamine / dichloromethane
2: nitric acid / -15 °C
With
nitric acid; triethylamine;
In
dichloromethane;
|
152628-01-8 Upstream products
-
301533-59-5
methyl 4-(n-butyrylamino)-3-methylbenzoate
-
3113-71-1
3-methyl-4-nitrobenzoic acid
-
18595-14-7
methyl 4-amino-3-methylbenzoate
-
24078-21-5
methyl 3-methyl-4-nitrobenzoate
152628-01-8 Downstream products
-
675882-71-0
3-methyl-4-butyrylamino-5-aminobenzoic acid methyl ester
-
152628-03-0
4-methyl-2-n-propyl-1H-benzimidazole-6-carboxylic acid
-
152628-00-7
4-methyl-2-propyl-1H-benzimidazole-6-carboxylic acid methyl ester
-
675882-83-4
4'-[4-methyl-6-(7-methyl-benzooxazol-2-yl)-2-propyl-benzoimidazol-1-ylmethyl]-biphenyl-2-carbonitrile
